3) For toluene (C6H5CH3): Calculate the degree of unsaturation Write down all possible structural elements to satisfy each degree of unsaturation List all signals you have determined from the functional group region of FTIR spectrum of your unknown. Make logical connection between your founding on FTIR spectrum and predictions based on the degree if unsaturation For 'H NMR spectrum make a table of peaks, their positions, integration and multiplicity Using multiplicity try to predict what groups are neighbors for each hydrogen Using the integration data calculate how many identical hydrogens are under each NMR peak By analyzing peak positions and comparing this data with your FTIR findings, try to predict what type of hydrogen environment cach peak represents Combining all analytical data and your calculations, predict the structure of your unknown. Show how this structure matches ALL your analytical data. If it only matches part of the data - you have a wrong structure. Agilent Technologies Sample ID:Group 5 unknown 29 Method Name:ATR 320 Sample Scans:32 User:FTIR UMES Background Scans:8 Date/Time:02/25/2020 4:03:52 PM Resolution:4 Range:4000 - 650 System Status: Good Apodization:Happ-Genzel File Location:C:\Users\Public Documents Agilent MicroLab Resultsl\Group 5 unknown 29_2020-02- 25T16-03-52.ar 92 soggme 04.95 91 90 3000 25.00 2000 Wavenumber(cm-1) Spinsolve magritek 1D CARBON WALTZ Amp HE 137.29 2772.625.284 128.67 2598.46 36.36 127.86 282.18 33.37 125.00 252.40 18.21 ppm 77.00 1955.10 7.182 20.91 422.22 12.51 Group 5 - unknown Toluene - Sample : Unknown Solvent: Chloroform 2020-02-25 10:16:50 1.2288 Acquisition Date: Number of scans : Acquisition time: Repetition time: Pulse angle: Center Frequency: Bandwidth: NOE amplitude: Decouple amplitude: 45 degrees 110 ppm 330.12 ppm -20.8 dB -20.8 dB Processing Resolution enhancement : Line broadening: Phasing: Baseline correction : None 1 HR PO -12.60 P1 = 0.00 Applied Meta data Instrument : Instrument type : Software version : User name: Datafolder: SPA1721 80 CARBON 1.15.5 1263 NMR students labs c:\projects\data\NMR students! abs2020102125\Unknown\2020 0225-101650-Unknown-1D CAR BON WALTZ 2020-02-25 08.04:28 0.40 HE 14.88 Hz 11842 Last Shim: Shim Enewidth Shimlinewidth Shim SNR 50% : 0.55%: INN WL TUNAHA 40 30 20 100 -1 0 240 230 230 210 200 150 160 170 100 150 140 130 120 110 100 90 80 70 60 50 magritek 1D PROTON Spinsolve Amp OSSZ LT 19 1008 0.005 29 HE 1.96 157.58 27430 Unknown - Toluene- Groups pom - Sample: Unknown Solvent: Chloroform 2020-02-25 10:11:17 Acquisition Date: Number of scans : Acquisition time: Repetition time: Pulse angle: 6.5535 15 5 90 degrees Processing Resolution enhancement: Line broadening: Phasing Baseline correction : 60 & 80 MHE: 0.0 LB +0.8 GB 0.2 Hz PO = 0.98 P1 - 200 Applied Meta data Instrument Instrument type : Software version: User name: Datafolder: SPA1721 BO CARBON 1.15.5.1263 NMR students labs c:\projects\data\NMR students abs\2020102125\Unknown 2020 0225-101117 Unknown-1D PRO TON 2020-02-25 08 04:28 0.40 Hz 14,88 H 11842 Last shim: Shimlinewidth Shimlinewidth Shim SNR: SOX: 0.55%: Integrals ppm range 2.24 - 1.77 6.37 - 6.01 723. 6.53 Normalized Absolu 34.17% 893.71 8.85 % 231.53 $6.97 1489.92 4 13 12 11 10